Molar masses
Rheology
Thermophysical properties
This platform brings together complementary equipment located in four of the research department laboratories and whose objective is the characterization of the structure and properties of polymers.
The available techniques enable different aspects to be addressed depending on the applications targeted.
Structural characterization:
- Chemical structure :
- liquid NMR spectrometry (LCPM)
- Pyrolysis coupled to gas chromatography-mass spectrometry (LERMaB)
- liquid NMR spectrometry (LCPM)
- Molar mass distribution :
- steric exclusion chromatography (LCPM, LERMaB)
- Average molar mass :
- capillary viscometry (LCPM)
Solution characterization :
- Conformation, dimensions :
- dynamic light scattering (LCPM)
- capillary viscometry (LCPM)
- Rheological behavior :
DSC-TGA equipment
Shock test apparatus (sheep-pendulum)
Solid DMA apparatus (Metravib +300N) for mechanical spectroscopy
Solid state characterization :
- Glass transition temperature, crystallization temperature, crystallinity rate :
- differential scanning calorimetry, classical and modulated (LCPM, LRGP)
- dynamic mechanical analysis apparatus, DMA (LRGP)
- Thermal stability under controlled atmosphere :
- thermogravimetric analysis (LERMaB, LRGP)
- Thermomechanical behavior :
- rheometers (LEMTA, LRGP)
- video-traction (LRGP)
- Shock testing apparatus (LRGP)
- Hardness measurement (LRGP, LERMaB)
- Three-point bending tests (LERMaB)
- Mechanical tests of intrinsic characterizations (polymers/Composites) :
- Instrumentation/sensors: Videoextensometry (measurement and control of tests), 3D image correlation (measurement of kinematic fields), Infrared imaging (measurement of thermal fields) (LEMTA)
- Mechanical stresses: Traction-Compression-Fatigue (MTS Hydraulic 25-100kN), Traction-Torsion (MTS Bionix 25kN), Harmonic (DMA+300N Acoem-Metravib), Fluage-Relaxation (LEMTA)
- Tensile or bending tests at temperature (LEMTA, LERMaB)
- Environmental stresses: Temperature tests (Ambient range +400°C) (LEMTA)
- Scientific calculation for the inverse estimation of intrinsic material properties by model(s)-metrology coupling (LEMTA)
- Water behaviour :
- Wettability measurement, sessile drop or tensiometer (LERMaB)
- gravimetry of water vapor adsorption (LERMaB)
- Aging under controlled conditions :
- Climatic chamber (LERMaB)
- QUV aging chamber (LERMaB)
Preparation of a sample for analysis by Py-GC-MS
Steric exclusion chromatography apparatus